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Anna University, India

 

Prof. Hassan Karimi-Maleh

University of Electronic Science
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Home > Archives > Vol. 8 No. 2(Published) > Original Research Article
ACE-5689

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2025-07-28

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Vol. 8 No. 2(Published)

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Original Research Article

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Copyright (c) 2025 Harianingsih Harianingsih, Catur Rini Widyastuti, Deni Fajar Fitriyana, Ari Dwi Nur Indriawan Musyono, Rizki Setiadi, Bunyamin Bunyamin, Maulana Dzaki Munawwar, Moh Luqman Hakim, Ade Mundari Wijaya, Dwi Novriadi

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How to Cite

Harianingsih, H., Widyastuti, C. R., Fitriyana, D. F., Indriawan Musyono, A. D. N., Setiadi, R., Bunyamin, B., … Novriadi, D. (2025). Analysis of reinforcement syntactic foam composite using K-15 microballoons. Applied Chemical Engineering, 8(2), ACE-5689. https://doi.org/10.59429/ace.v8i2.5689
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Analysis of reinforcement syntactic foam composite using K-15 microballoons

Harianingsih Harianingsih

Department of Chemical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Catur Rini Widyastuti

Department of Chemical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Deni Fajar Fitriyana

Department of Mechanical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Ari Dwi Nur Indriawan Musyono

Department of Mechanical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Rizki Setiadi

Department of Mechanical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Bunyamin Bunyamin

Department of Mechanical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Maulana Dzaki Munawwar

Department of Chemical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Moh Luqman Hakim

Department of Chemical Engineering, Faculty of Engineering, Universitas Negeri Semarang, Kampus Sekaran Gunungpati, Semarang 50229, Indonesia

Ade Mundari Wijaya

Center for Polymer Technology - National Research and Innovation Agency, Kawasan Puspitek Serpong, South Tangerang, Banten 15314, Indonesia

Dwi Novriadi

Center for Polymer Technology - National Research and Innovation Agency, Kawasan Puspitek Serpong, South Tangerang, Banten 15314, Indonesia


DOI: https://doi.org/10.59429/ace.v8i2.5689


Keywords: density; flexural; K-15 microballons; syntactic foam composite


Abstract

Syntactic foam composites are used in the aerospace industry, one of which is for buoys because they are lightweight materials that have flexural strength and are resistant to corrosion. This study aims to determine the flexural properties and morphologies structure of syntactic foam composite with K-15 microballoons filler mixed by epoxy resin. Syntactic foam is a lightweight material used in the maritime sector for buoys to make them float easily in water. Variations of K-15 microballoons of 10%, 20%, 30%, 40% and 50% volume of syntactic foam composite. Flexural strength determinated using ASTM D790 and morphologie structure determined with scanning electron microscope (SEM). The addition of X-15 microballoons can reduce flexural strength compared to pure epoxy. Flexural strength in pure epoxy in the form of stress, elastic modulus, and strain each produces values of 71.28, 2928.47 MPa, 2.75 MPa. The highest impact is seen in the addition of 50% K-15 microballoons with stress, elastic modulus, strain and density values of 18.59, 1406.03 MPa, 1.43 MPa and 0.63 kgm-3 respectively. SEM analysis shows that plain epoxy has a smooth surface without voids, whereas with the addition of K-15 microballoons, voids appear on the surface of the syntactic foam composite.


References

[1]. Anirudh, S., Jayalakshmi, C. G., Anand, A., Kandasubramanian, B., & Ismail, S. O. Epoxy/hollow glass microsphere syntactic foams for structural and functional application-A review. European Polymer Journal 2022: 171, 111163. https://doi.org/10.1016/j.eurpolymj.2022.111163

[2]. DSouza, G. C., Ng, H., Charpentier, P., & Xu, C. C. Recent developments in biobased foams and foam composites for construction applications. ChemBioEng Reviews 2024; 11(1), 7-38. https://doi.org/10.1002/cben.202300014

[3]. Mooij, E.Thermal Protection Systems. In Re-entry Systems 2024; 1085-1258. https://doi.org/10.1007/978-3-031-62174-1_10

[4]. Munawar, M. D., Hakim, M. L., Wijaya, A. M., & Novriadi, D. Analysis of Voids and Porosity and Its Influence on The Quality of Syntactic Foam Composites. Sainteknol: Jurnal Sains dan Teknologi 2023; 21(2), 70-80. https://doi.org/10.15294/sainteknol.v21i2.49530

[5]. Rajak, D. K., & Gupta, M. An Insight Into Metal Based Foams. Singapore, Springer 2020; 10, 978-981. https://doi.org/10.1007/978-981-15-9069-6

[6]. Tagliavia, G., Porfiri, M., & Gupta, N. Vinyl ester—glass hollow particle composites: dynamic mechanical properties at high inclusion volume fraction. Journal of Composite Materials 2009; 43(5), 561-582. https://doi.org/10.1177/0021998308097683

[7]. Hamonangan, W. M., Lee, S., Choi, Y. H., Li, W., Tai, M., & Kim, S. H. Microballoons: Osmotically-inflated elastomer shells for ultrafast release of encapsulants and mechanical energy. Journal of Colloid and Interface Science 2024; 668, 272-281. https://doi.org/10.1016/j.jcis.2024.04.146

[8]. Ullas, S., Hausfeld, L., Cutler, A., Eisner, F., & Formisano, E. Neural correlates of phonetic adaptation as induced by lexical and audiovisual context. Journal of Cognitive Neuroscience 2020; 32(11), 2145-2158. https://doi.org/10.1162/jocn_a_01608

[9]. John, B., & Nair, C. R. 2022. Thermosetting polymer based syntactic foams: an overview. Handbook of thermoset plastics 2022; 801-832. https://doi.org/10.1016/B978-0-12-821632-3.00020-8

[10]. Jayaprakash, D., Niranjan, K., & Vinod, B. Studies on mechanical and microstructural properties of aluminium hybrid composites: influence of SiC/Gr particles by double stir-casting approach. Silicon 2023; 15(3), 1247-1261. https://doi.org/10.1007/s12633-022-02106-7

[11]. Waddar, S., Pitchaimani, J., Doddamani, M., & Barbero, E. Buckling and vibration behaviour of syntactic foam core sandwich beam with natural fiber composite facings under axial compressive loads. Composites Part B: Engineering 2019; 175, 107133. https://doi.org/10.1016/j.compositesb.2019.107133

[12]. Bell, M. A., Becker, K. P., & Wood, R. J. Injection molding of soft robots. Advanced Materials Technologies 2022; 7(1), 2100605.https://doi.org/10.1002/admt.202100605

[13]. Fernandes, F., Manari, S., Aguayo, M., Santos, K., Oey, T., Wei, Z., ... & Sant, G. On the feasibility of using phase change materials (PCMs) to mitigate thermal cracking in cementitious materials. Cement and Concrete Composites 2014; 51, 14-26.https://doi.org/10.1016/j.cemconcomp.2014.03.003

[14]. Meng, J., Jiao, Y., Xiao, M., Liu, Z., & Chen, R. 2024. Effect of shear span-to-depth ratio on flexural and fracture behaviors of reinforced UHPMC beams based on four-point bending test and acoustic emission monitoring. Journal of Building Engineering 2024; 96, 110457. https://doi.org/10.1016/j.jobe.2024.110457

[15]. Wulandari, R., Radini, F. A., Yunus, M., Arti, D. K., Harianingsih, Rusmana, D., & Pratama, A. 2023. Comparative Study of Commercial Glass Fiber-Reinforced Polyester Composite Beams: Thermal Behavior and Durability to QUV Exposure. Journal of The Institution of Engineers (India): Series D 2023; 1-10. https://doi.org/10.1007/s40033-023-00599-z

[16]. Nguyen, K. T., Ahn, N., Le, T. A., & Lee, K. Theoretical and experimental study on mechanical properties and flexural strength of fly ash-geopolymer concrete. Construction and Building Materials 2016; 106, 65-77. https://doi.org/10.1016/j.conbuildmat.2015.12.033

[17]. Errichiello, F., Amato, D., Penati, M., & Di Maio, E. Foam density measurement using a 3D scanner. Journal of Cellular Plastics 2024; 60(5-6), 283-299. https://doi.org/10.1177/0021955X241281880

[18]. Baer, D. R., Cant, D. J., Castner, D. G., Ceccone, G., Engelhard, M. H., Karakoti, A. S., & Müller, A. Preparation of nanoparticles for surface analysis. In Characterization of Nanoparticles 2020; pp. 295-347. https://doi.org/10.1016/B978-0-12-814182-3.00018-3

[19]. Xing, B., Du, Y., Fang, C., Sun, H., Lyu, Y., & Fan, W. Particle morphology of mineral filler and its effects on the asphalt binder-filler interfacial interaction. Construction and Building Materials 2022; 321, 126292. https://doi.org/10.1016/j.conbuildmat.2021.126292

[20]. Afolabi, O. A., Kanny, K., & Mohan, T. P. Analysis of particle variation effect on flexural properties of hollow glass microsphere filled epoxy matrix syntactic foam composites. Polymers 2022; 14(22), 4848. https://doi.org/10.3390/polym14224848

[21]. Bakshi, M. S., & Kattimani, S. Study of mechanical and dynamic mechanical behavior of halloysite nanotube‐reinforced multiscale syntactic foam. Journal of Applied Polymer Science 2021; 138(7), 49855. https://doi.org/10.1002/app.49855

[22]. Wang, Y., Zhu, M., & Zhu, X. X. 2021. Functional fillers for dental resin composites. Acta biomaterialia 2021; 122, 50-65. https://doi.org/10.1016/j.actbio.2020.12.001

[23]. Dando, K. R., Cross, W. M., Robinson, M. J., & Salem, D. R. Characterization of mixture epoxy syntactic foams highly loaded with thermoplastic and glass microballoons. Journal of Composite Materials 2019; 53(13), 1737-1749. https://doi.org/10.1177/0021998317716267

[24]. Wang, Y., Ya, B., Zhou, B., Meng, L., & Zhang, X. Numerical simulation of the mechanical properties of a carbon‐fiber‐reinforced hollow glass microsphere–epoxy syntactic foam. Journal of Applied Polymer Science 2019; 136(8), 47083. https://doi.org/10.1002/app.47083

[25]. Patil, A. N., Kubade, P. R., & Kulkarni, H. B. Mechanical properties of hybrid glass micro balloons/fly ash cenosphere filled vinyl ester matrix syntactic foams. Materials Today: Proceedings 2020; 22, 1994-2000. https://doi.org/10.1016/j.matpr.2020.03.165

[26]. Li, Y., Huang, X., Zeng, L., Li, R., Tian, H., Fu, X., ... & Zhong, W. H. A review of the electrical and mechanical properties of carbon nanofiller-reinforced polymer composites. Journal of Materials Science 2019; 54, 1036-1076. https://doi.org/10.1007/s10853-018-3006-9

[27]. Wijaya, A. M., Ardhyananta, H., Hidayat, M. I. P., Rifathin, A., Laksmono, J. A., Novriadi, D., & Yunus, M. Mechanical Properties, Density, and Morphology Analysis of Strong and Lightweight Microfibril Cellulose Reinforced Epoxy/Micro Balloon Hybrid Composites. Journal of The Institution of Engineers (India): Series D 2024; 1-12. https://doi.org/10.1007/s40033-024-00796-4



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